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ETPU Precursor Pelletizing Solution

Reactive extrusion and uniform micro-pellet production for downstream expanded-TPU bead and footwear development.

Process configuration

Engineered Precursor Chemistry for High-Energy-Return Popcorn Midsoles

Reactive extrusion and uniform micro-pellet production for downstream expanded-TPU bead and footwear development.

Equipment and process scope

Liquid feed preparation, reactive extrusion, melt pumping and micro-pelletizer with drying interfaces. Supercritical-gas expansion and bead molding equipment are separately defined.

Validation and production planning

This line produces unexpanded TPU precursor pellets. Supercritical expansion and steam-chest molding are downstream stages, not proven functions of the pelletizer. Rebound, expansion ratio and foam density refer to specified downstream samples. Extrusion pressure and supercritical vessel pressure are distinct. ASTM D2632 covers solid rubber and excludes cellular rubber; confirm an appropriate validated method for the cellular ETPU sample before using the reported rebound comparison.

Liquid feed preparation, reactive extrusion, melt pumping and micro-pelletizer with drying interfaces. Supercritical-gas expansion and bead molding equipment are separately defined. This line produces unexpanded TPU precursor pellets. Supercritical expansion and steam-chest molding are downstream stages, not proven functions of the pelletizer. Rebound, expansion ratio and foam density refer to specified downstream samples. Extrusion pressure and supercritical vessel pressure are distinct. ASTM D2632 covers solid rubber and excludes cellular rubber; confirm an appropriate validated method for the cellular ETPU sample before using the reported rebound comparison.Generated concept illustration for process discussion; not a photograph of the specified machine, a customer facility or a delivered project.

Process configuration

Turnkey ETPU Precursor Granulation Process

Configuration sequence from the supplied brief. Material, tool, pressure/temperature basis and complete line balance require verification. This line produces unexpanded TPU precursor pellets. Supercritical expansion and steam-chest molding are downstream stages, not proven functions of the pelletizer. Rebound, expansion ratio and foam density refer to specified downstream samples. Extrusion pressure and supercritical vessel pressure are distinct. ASTM D2632 covers solid rubber and excludes cellular rubber; confirm an appropriate validated method for the cellular ETPU sample before using the reported rebound comparison.

01

Four-Stream Closed-Loop Mass-Flow Feeding

Supplied process reference: Low-crystallinity PCL polyols, PTMEG, molten pure MDI, and extenders are metered at 85°C into the extruder throat under nitrogen.

LIQUID DOSING TOLERANCE ±0.15%; NITROGEN BLANKET 0.05 MPA; CONFIRM FOR SELECTED MATERIAL AND TOOLING
02

Controlled-Crystallinity Twin-Screw Polymerization

Supplied process reference: Reactants advance through an L/D = 54 barrel, where low-shear blocks guide molecular weight growth to tailor hard-segment domains.

BARREL L/D = 54; TEMPERATURE 170–205°C; CONFIRM FOR SELECTED MATERIAL AND TOOLING
03

Gear Pump Pressure Stabilization & Fine Filtration

Supplied process reference: An oil-jacketed melt pump stabilizes delivery pressure at 15.0 MPa, passing melt through a 250-mesh hydraulic screen changer.

MELT PRESSURE 15.0 MPA; SCREEN MESH 250-MESH; CONFIRM FOR SELECTED MATERIAL AND TOOLING
Process configuration

Reference Solution Engineering Envelope

Supplied configuration and validation references; material/component results are separate from equipment ratings.

ParameterValue / UnitApplicable Configuration / Conditions
Continuous Production Output200.0 to 600.0 kg/hourHigh-torque co-rotating twin-screw extruder with gear pump; supplied configuration or material target, pending the applicable original records
Precursor Bead Diameter Profile1.2 mm ± 0.05 mmMicro-orifice carbide die plate (0.8–1.2 mm holes); supplied configuration or material target, pending the applicable original records
Supercritical Autoclave Expansion4.0 to 6.0 Times (sc-CO₂)Physical autoclaving at 12 MPa and 125°C; supplied configuration or material target, pending the applicable original records
Molded Sole Ball ReboundReported cellular-sample rebound; method pending reviewASTM D2632 excludes cellular rubber; establish an appropriate validated method and original ETPU sample record
Expanded Bead Specific Gravity0.15 to 0.22 g/cm³Water displacement density measurement; supplied configuration or material target, pending the applicable original records
Precursor Residual MoistureLess than 0.02% (200 ppm)High-speed centrifugal spin dryer with fluidized bed; supplied configuration or material target, pending the applicable original records
This line produces unexpanded TPU precursor pellets. Supercritical expansion and steam-chest molding are downstream stages, not proven functions of the pelletizer. Rebound, expansion ratio and foam density refer to specified downstream samples. Extrusion pressure and supercritical vessel pressure are distinct. ASTM D2632 covers solid rubber and excludes cellular rubber; confirm an appropriate validated method for the cellular ETPU sample before using the reported rebound comparison.

Core Equipment for This Solution

Liquid feed preparation, reactive extrusion, melt pumping and micro-pelletizer with drying interfaces. Supercritical-gas expansion and bead molding equipment are separately defined.

Core Advantages of Haifeng ETPU Systems

Configured equipment functions and interfaces for the selected material and tooling.

Extreme > 68% Energy Return

Supplied configuration function: Tailored soft-segment chemistry minimizes hysteretic mechanical energy loss under cyclic running strikes. Project-dependent performance requires validation.

1.2 mm Mini-Pellet Uniformity

Supplied configuration function: Micro-orifice underwater cutting yields identical bead masses, preventing irregular expansion in autoclaves. Project-dependent performance requires validation.

4–6x Supercritical Expansion

Supplied configuration function: Precursor formulation maximizes sc-CO₂ gas uptake, yielding ultra-lightweight densities (0.15– 0.22 g/cm^3). Project-dependent performance requires validation.

High-Pressure Non-Freezing Die

Supplied configuration function: Advanced ceramic internal thermal barriers prevent micro-orifices from freezing in water, ensuring steady runs. Project-dependent performance requires validation.

Related review draft

Related Project Draft

An anonymous project brief from the supplied document. Original attribution, dates, acceptance and outcome records require verification before public use.

Review Project
Planning questions

Frequently Asked Questions

Why can't standard 3.0 mm TPU pellets be used for high-end ETPU midsoles? +
Large beads expand into coarse popcorn shapes that create voids and uneven flexure when molded into shoe midsoles. Confirm the applicable formulation, geometry and original test records. This line produces unexpanded TPU precursor pellets. Supercritical expansion and steam-chest molding are downstream stages, not proven functions of the pelletizer. Rebound, expansion ratio and foam density refer to specified downstream samples. Extrusion pressure and supercritical vessel pressure are distinct. ASTM D2632 covers solid rubber and excludes cellular rubber; confirm an appropriate validated method for the cellular ETPU sample before using the reported rebound comparison.
How does the machine prevent die-hole freeze-offs with small 0.8 mm holes? +
The die incorporates internal thermal oil channels and ceramic insulation, keeping metal faces hot in cool water. Confirm the applicable formulation, geometry and original test records. This line produces unexpanded TPU precursor pellets. Supercritical expansion and steam-chest molding are downstream stages, not proven functions of the pelletizer. Rebound, expansion ratio and foam density refer to specified downstream samples. Extrusion pressure and supercritical vessel pressure are distinct. ASTM D2632 covers solid rubber and excludes cellular rubber; confirm an appropriate validated method for the cellular ETPU sample before using the reported rebound comparison.
What is the ideal gas medium for expanding these precursor beads? +
Supercritical carbon dioxide (sc-CO₂) at 10–14 MPa and 120–130°C yields the finest microcellular open/closed structures. Confirm the applicable formulation, geometry and original test records. This line produces unexpanded TPU precursor pellets. Supercritical expansion and steam-chest molding are downstream stages, not proven functions of the pelletizer. Rebound, expansion ratio and foam density refer to specified downstream samples. Extrusion pressure and supercritical vessel pressure are distinct. ASTM D2632 covers solid rubber and excludes cellular rubber; confirm an appropriate validated method for the cellular ETPU sample before using the reported rebound comparison.
Can these precursor beads be colored during the reactive extrusion process? +
Yes, auxiliary liquid colorant pumps can inject pigments directly into the melt before the screen changer. Confirm the applicable formulation, geometry and original test records. This line produces unexpanded TPU precursor pellets. Supercritical expansion and steam-chest molding are downstream stages, not proven functions of the pelletizer. Rebound, expansion ratio and foam density refer to specified downstream samples. Extrusion pressure and supercritical vessel pressure are distinct. ASTM D2632 covers solid rubber and excludes cellular rubber; confirm an appropriate validated method for the cellular ETPU sample before using the reported rebound comparison.

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